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Study on the Selective Surface Modification of Injection Mold Steels by Laser Materials Processing: Relationship Between AlN Formation and Surface Hardening During Laser Nitriding
레이저 가공 기반 사출 금형강의 선택적 표면 개질 연구: 레이저 나이트라이딩에 따른 AlN 형성 및 경화 거동
Eun-Joon Chun, Changkyoo Park, Wonah Park
천은준, 박창규, 박원아
Korean J. Met. Mater. 2020;58(1):32-40.   Published online 2019 Dec 12
DOI: https://doi.org/10.3365/KJMM.2020.58.1.32

Abstract
Laser surface heat treatment and laser nitriding processes were applied using selective surface modification techniques to investigate phase transformation, microstructural evolution, and surface hardening behaviors for two types of plastic injection mold steels, AISI 1045 and P21. During laser surface heat treatment, a 245% hardness increase compared to that of..... More

                   Web of Science 4  Crossref 4
Effect of Surface Roughness on the Formation of Nano-to-Mirco Patterns Using Pattern Transfer Printing
나노-마이크로 패턴의 형성에 미치는 기판의 표면 거칠기 영향
Tae Wan Park, Myunghwan Byun, Hyunsung Jung, Woon Ik Park
박태완, 변명환, 정현성, 박운익
Korean J. Met. Mater. 2020;58(1):26-31.   Published online 2019 Dec 12
DOI: https://doi.org/10.3365/KJMM.2020.58.1.26

Abstract
The ability to form high quality nano-/micro- patterns is very important for the nanofabrication of high-density electronic devices. However, remaining challenges have yet to be resolved, including low quality roughness, low pattern resolution, and the highly complex process. In this study, we suggest a novel and simple method for creating..... More

                   Web of Science 1
Effect of Heat Treatment on Mechanical Properties and Energy Absorption Capacity of 7003 Aluminum Alloy
7003 알루미늄 합금의 기계적 성질 및 에너지 흡수능에 미치는 열처리 조건의 영향
Hee-Ju Kim, Jeki Jung, Su-Hyeon Kim, Cha-Yong Lim, Yoon Suk Choi
김희주, 정제기, 김수현, 임차용, 최윤석
Korean J. Met. Mater. 2020;58(1):7-16.   Published online 2019 Dec 12
DOI: https://doi.org/10.3365/KJMM.2020.58.1.7

Abstract
The effects of heat treatment conditions on the mechanical properties and energy absorption capacity of 7003 (Al-6Zn-0.6Mg) aluminum alloy were studied. The extruded material was heat treated at various temperatures to prepare annealed or aged specimens. Tensile tests, hardness measurements, electron backscatter diffraction characterizations, and differential scanning calorimeter analyses were..... More

                   Web of Science 6  Crossref 6
Study on the Effect of the Thiourea on Nano-Mechanical Properties and Microstructures of the Electroformed Thin Ni-P Foil
Moo Young Jung, Chang Su Nam, Byung-Sik Lee, Yong Choi
Korean J. Met. Mater. 2020;58(1):1-6.   Published online 2020 Jan 1
DOI: https://doi.org/10.3365/KJMM.2020.58.1.1

Abstract
The effect of thiourea on the nano-mechanical and chemical properties of Ni-P foil was studied to develop a high performance Ni-P deposit for automobile and machinery parts. The Ni-P deposit was prepared by electroforming in a modified sulphate bath with different amounts of thiourea. Chemical analysis of the electrodeposited Ni-P..... More

                   Web of Science 3  Crossref 4
Demonstration Testing of Boiler Tubes in a Clean Power Test-Bed Plant
Yeon kwan Kang, Yinsheng He, Han-Sang Lee, Beom-Soo Kim, Liming Xu, Keesam Shin
Korean J. Met. Mater. 2019;57(12):817-827.   Published online 2019 Nov 22
DOI: https://doi.org/10.3365/KJMM.2019.57.12.817

Abstract
The use of locally developed high performance alloys in power plants has become essential in the past ten years. Application of these alloys has been difficult because of a shortage of field demonstration testing, and the lack of lab-based test data. In this work, three types of locally developed heat..... More

                   Crossref 3
Synthesis and Thermoelectric Properties of Partially Double-Filled Skutterudites (La1−zYbz)0.8Fe4−xCoxSb12
Ye-Eun Cha, Il-Ho Kim
Korean J. Met. Mater. 2019;57(12):801-807.   Published online 2019 Nov 22
DOI: https://doi.org/10.3365/KJMM.2019.57.12.801

Abstract
Partially double-filled skutterudites were prepared via encapsulated melting and hot pressing processes. The skutterudite phase was successfully synthesized through partial double filling of La/Yb and substitution of Co. A small quantity of secondary phase (marcasite FeSb2) was formed, but its formation was suppressed by increasing Co charge compensation. The marcasite..... More

                   Crossref 2
Comparison of the Extraction and Stripping Behavior of Iron (III) from Weak Acidic Solution Between Ionic Liquids and Commercial Extractants
Thanh Tuan Tran, Mudassir Iqbal, Man Seung Lee
Korean J. Met. Mater. 2019;57(12):787-794.   Published online 2019 Nov 22
DOI: https://doi.org/10.3365/KJMM.2019.57.12.787

Abstract
Fe(III) can be easily extracted from weak acidic solutions by organophosphorus extractants, but stripping a large amount of Fe(III) from the loaded extractants is very difficult. The extraction and stripping of Fe(III) from 2 pH chloride and sulfate solutions was performed with ionic liquids(ILs) and organophosphorus acidic extractants, and the..... More

                   Crossref 10
Analysis of White Spots Formation on Autogeneous TIG Welds of Cryogenic Fe-36%Ni Steels
극저온용 Fe-36%Ni강 자동 용접부의 White spot 생성 원인 분석
Hee-keun Lee
이희근
Korean J. Met. Mater. 2019;57(12):771-777.   Published online 2019 Nov 22
DOI: https://doi.org/10.3365/KJMM.2019.57.12.771

Abstract
Fe-36%Ni steels have a much lower thermal expansion coefficient than stainless steels and aluminum alloys for low temperature. They also have moderately high strength and good toughness at cryogenic temperatures because of its stable austenite phase. These excellent low temperature characteristics make this alloy attractive for cryogenic applications such as..... More

                   Crossref 3
Microstructure and Mechanical Properties of Continuous Welded 50N Rail
Wookjin Choi, Min Ji Song, Nam-Hyoung Lim, Soo Yeol Lee
Korean J. Met. Mater. 2019;57(12):755-763.   Published online 2019 Dec 5
DOI: https://doi.org/10.3365/KJMM.2019.57.12.755

Abstract
Rails are subjected to repeated stresses due to wheel-rail contact during train service. Rails under stress conditions undergo microstructural changes, and these cause degradations of the structural integrity and lifetime of rails. In this study, three different rails (newly-manufactured rail, newly-manufactured head-hardened rail, and worn (used) rail) were compared to..... More

                
Investigation of Structure-Property Relations in Porous Metals Using Finite Element Simulation
유한요소해석을 활용한 다공 금속의 구조-물성 관계 연구
Dongmyung Jung, Yongwoo Kwon
정동명, 권용우
Korean J. Met. Mater. 2019;57(11):747-754.   Published online 2019 Nov 5
DOI: https://doi.org/10.3365/KJMM.2019.57.11.747

Abstract
A porous material can be regarded as a mixture of pores and solid phases, with effective thermal and mechanical properties that significantly differ from those of its base material. Material effective properties depend greatly on the structure and porosity. The effective properties of materials with different pore structures can vary..... More

                   Crossref 1
Recovery of Cadmium in Nickel-Cadmium Leaching Solution by Sulfide Precipitation Method
폐니켈-카드뮴 침출용액으로부터 황화물 침전법을 이용한 카드뮴 회수에 대한 연구
Il-Jeong Park, Dae-Weon Kim, Min-Jun Kim, Hang-Chul Jeong
박일정, 김대원, 김민준, 정항철
Korean J. Met. Mater. 2019;57(11):726-731.   Published online 2019 Nov 5
DOI: https://doi.org/10.3365/KJMM.2019.57.11.726

Abstract
A large amount of waste nickel-cadmium batteries are being produced, and various studies have been conducted to recover the valuable metals contained in the batteries. Solvent extraction is mainly used to recover nickel and cadmium, but that method has economic and environmental problems. In this study, to solve these problems,..... More

                   Web of Science 1  Crossref 1
Study on the Effect of the Localized Electrode Degradation on Weldability During an Electrode Life Test in Resistance Spot Welding of Ultra-High Strength Steel
초고강도강 저항 점용접 연속타점시 전극의 국부적 합금화 현상이 용접품질 저하에 미치는 영향 연구
Jae-Won Kim, Siva Prasad Murugan, Nam Hyun Kang, Yeong-Do Park
김재원, Siva Prasad Murugan, 강남현, 박영도
Korean J. Met. Mater. 2019;57(11):715-725.   Published online 2019 Nov 5
DOI: https://doi.org/10.3365/KJMM.2019.57.11.715

Abstract
Evaluation of electrode degradation in resistance spot welding of 1180TRIP steel was carried out through an electrode life test, and weldability testing was performed by the measurement of the nugget size, the peak load analysis and the measurement of the electrode tip size at 30 intervals. Analysis of the change..... More

                   Web of Science 7  Crossref 6
Fabrication of Open-Pored Titanium Foam for Biomedical Implants
생체의료 임플란트용 개기공 티타늄 다공체 제조
Gyeong-Uk Kim, Jin Man Jang, Yong-Dae Kim, Jae-Chul Lee, Wonsik Lee
김경욱, 장진만, 김용대, 이재철, 이원식
Korean J. Met. Mater. 2019;57(10):679-687.   Published online 2019 Sep 6
DOI: https://doi.org/10.3365/KJMM.2019.57.10.679

Abstract
Open-pored metal foams have been partly used for orthopedic or dental applications because of their good bone ingrowth behavior and low elastic modulus. In this paper, we report a method that can produce open-pored Ti foams using a technique that combines the powder injection molding process and feedstocks containing expandable..... More

                   Web of Science 3  Crossref 3
Improvement of the Hydrogen-Release Features of Mg-Graphene Composite by Adding Nickel via Reactive Ball Milling
Eunho Choi, Young Jun Kwak, Myoung Youp Song
Korean J. Met. Mater. 2019;57(10):663-672.   Published online 2019 Sep 6
DOI: https://doi.org/10.3365/KJMM.2019.57.10.663

Abstract
The dehydrogenation rates of graphene-added Mg (named Mg-5graphene) were very low at 573 K and 593 K. Ni was added to increase the dehydrogenation rates of graphene-added Mg. Samples (designated as Mg-2.5Ni-2.5graphene) with a composition of 95 wt% Mg + 2.5 wt% Ni + 2.5 wt% graphene were prepared by..... More

                   Web of Science 7  Crossref 6
A Study on the Separation and Concentration of Li from Li-Containing Waste Solutions by Electrodialysis
리튬함유 폐액으로부터 전기투석에 의한 리튬의 분리·농축 연구
Jueun Lee, Hongil So, Yeonchul Cho, Inhwan Jang, Jaewoo Ahn, Jaeheon Lee
이주은, 소홍일, 조연철, 장인환, 안재우, 이재헌
Korean J. Met. Mater. 2019;57(10):656-662.   Published online 2019 Sep 6
DOI: https://doi.org/10.3365/KJMM.2019.57.10.656

Abstract
Electrodialysis was used to develop a highly efficient process for concentrating and recovering Li from the Li-containing waste solution that is generated after recovering Co and Ni from a leach solution of waste cathode materials of Li ion batteries. The optimum conditions were investigated by comparing the concentration of Li..... More

                   Web of Science 4  Crossref 6
High-Temperature Corrosion of Ti-44Al-6Nb-2Cr-0.3Si-0.1C Alloy in 0.2%SO2/Ar Gas
Ti-44Al-6Nb-2Cr-0.3Si-0.1C 합금의 0.2%SO2/Ar가스에서의 고온부식
Shi Yuke, Xiao Xiao, Seong Woong Kim, Jae Keun Hong, Junhee Hahn, Dong Bok Lee
Shi Yuke, Xiao Xiao, 김성웅, 홍재근, 한준희, 이동복
Korean J. Met. Mater. 2019;57(10):648-655.   Published online 2019 Sep 23
DOI: https://doi.org/10.3365/KJMM.2019.57.10.648

Abstract
Cast Ti–44Al–6Nb–2Cr–0.3Si–0.1C alloy having good air-oxidation resistance was corroded under 1 atm of flowing 0.2%SO2/Ar gas at 900-1100 oC for 50-300 h in order to examine its corrosion behavior in a SO2-containing environment, because SO2 is an industrially important by-product in the field of combustion and processing of fossil fuels...... More

                   Web of Science 1  Crossref 1
Selective Extraction of Cu(II) from Sulfuric Acid Leaching Solutions of Spent Lithium Ion Batteries Using Cyanex 301
폐리튬 이차전지 황산침출용액에서 Cyanex 301에 의한 구리(II)의 선택적 추출
Se Ah Lee, Man Seung Lee
이세아, 이만승
Korean J. Met. Mater. 2019;57(9):596-602.   Published online 2019 Aug 21
DOI: https://doi.org/10.3365/KJMM.2019.57.9.596

Abstract
Spent lithium ion batteries contain cobalt, copper, lithium, manganese and nickel. Recovery of these metals with high purity from spent lithium ion batteries is of importance. A sulfuric acid solution is generally employed for the treatment of spent lithium ion batteries, but it is difficult to separate these metal ions..... More

                   Web of Science 7  Crossref 8
Adsorption of Pd(II) onto Zr(IV) Based Metal-Organic Framework UIO-66-NH2 from Hydrochloric Acid Solution
염산 용액에서 지르코늄(IV)계 금속-유기물 구조체 UIO-66-NH2의 팔라듐(II) 흡착
Hyeong Hun Ahn, Man Seung Lee
안형훈, 이만승
Korean J. Met. Mater. 2019;57(9):589-595.   Published online 2019 Aug 21
DOI: https://doi.org/10.3365/KJMM.2019.57.9.589

Abstract
Metal-organic frameworks are used in many applications, such as gas separation, catalysis, and the synthesis of nanomaterials. Metal-organic frameworks show superior stability at high temperature, which makes them potentially useful for the adsorption of metal ions from leaching solutions at high temperature. In this work, UIO-66-NH2, a zirconium(IV) based metal-organic..... More

                   Web of Science 1  Crossref 1
Optimization of the CMP Process with Colloidal Silica Performance for Bulk AlN Single Crystal Substrate
Hyo Sang Kang, Joo Hyung Lee, Jae Hwa Park, Hee Ae Lee, Won Il Park, Seung Min Kang, Sung Chul Yi
Korean J. Met. Mater. 2019;57(9):582-588.   Published online 2019 Aug 21
DOI: https://doi.org/10.3365/KJMM.2019.57.9.582

Abstract
Chemical mechanical polishing (CMP) of bulk AlN was performed with colloidal silica slurry at pH 9 for different times. The result shows that colloidal silica slurry at pH 9, which has the relatively high surface charge of -50.7 mV is most stable, and it was selected as chemically optimum condition..... More

                   Web of Science 4  Crossref 3
High-Temperature Oxidation of Fe-12Cr-0.3C-4Mn-(13-15)Cu Composite Alloys
Min Jung Kim, Sang-Hwan Bak, Junhee Hahn, Seon Jin Kim, Dong Bok Lee
Korean J. Met. Mater. 2019;57(9):575-581.   Published online 2019 Aug 21
DOI: https://doi.org/10.3365/KJMM.2019.57.9.575

Abstract
Alloys of Fe-12Cr-0.3C-4Mn-(13, 14, 15)Cu (wt%) were cast using an induction furnace. They were structurally heterogeneous composites that consisted of a relatively stiff α-Fe matrix and a soft (Cu, Mn)-rich secondary phase. They were developed as self-lubricating, wear-resistant metals. Since the formation of oxides plays an important role in wear,..... More

                   Web of Science 4  Crossref 6
Effect of Annealing Temperature on the Shape Memory Properties of Ti-44.5Ni-5Cu and Ti-45.2Ni-5Cu(at%) Alloys
Ti-44.5Ni-5Cu 및 Ti-45.2Ni-5Cu(at%) 합금의 형상기억특성에 미치는 어닐링온도의 영향
Jae Il Kim, Kwang Sun Hwang
김재일, 황광선
Korean J. Met. Mater. 2019;57(9):562-568.   Published online 2019 Aug 21
DOI: https://doi.org/10.3365/KJMM.2019.57.9.562

Abstract
The effect of annealing temperature on shape memory properties in the Ti-44.5Ni-5Cu and Ti-45.2Ni-5Cu(at%) alloys was investigated by differential scanning calorimeter (DSC) and tensile testing. The martensitic transformation temperature of Ti-44.5Ni-5Cu(at%) increased from 308K to 324K with increasing annealing temperature and did not change with further increasing annealing temperature. This..... More

                   Web of Science 2  Crossref 2
Evaluation of Dynamic Precipitation in Extruded Mg-Zn Alloy
Mg-Zn합금의 압출 공정 중 동적 석출 거동에 대한 고찰
Guang Zhe Li, Min Young Na, Hye Jung Chang, Pil Ryung Cha, Yu Chan Kim, Hyun Kwang Seok
이광철, 나민영, 장혜정, 차필령, 김유찬, 석현광
Korean J. Met. Mater. 2019;57(9):555-561.   Published online 2019 Aug 21
DOI: https://doi.org/10.3365/KJMM.2019.57.9.555

Abstract
The dynamic precipitation evolution of Mg-3 wt% Zn alloy during extrusion was evaluated in this study. Precipitation evolution during aging has been well investigated for the Mg-Zn alloy, which is known as static precipitation. However, little attention has been given to dynamic precipitation in Mg-Zn alloy. In order to evaluate..... More

                   Crossref 1
Effect of In-Situ Post Heating on Repairing STS316L Built by Laser Powder Bed Fusion Using Direct Energy Deposition
레이저로 적층 제조된 STS316L에 대한 직접에너지적층 응용 보수 시 공정 중 후열처리(In-Situ Post Heating) 효과
Wook Jin Oh, Yong Son, Do Sik Shim
오욱진, 손용, 심도식
Korean J. Met. Mater. 2019;57(8):543-553.   Published online 2019 Jul 11
DOI: https://doi.org/10.3365/KJMM.2019.57.8.543

Abstract
The repairing parts were fabricated by PBF (powder bed fusion) using direct energy deposition (DED), interfacial cracks can occur at the interface between the substrate and the area to be repaired. Such interfacial defects are due to the thermal stress induced by the temperature gradient which results from repeated melting..... More

                   Web of Science 5  Crossref 5
Computational Design of Highly Efficient and Robust Hole Transport Layers in Perovskite Solar Cells
페로브스카이트 태양전지의 최적 정공수송층 물질 및 구조 탐색 시뮬레이션
Jiyoung Jeong, Dongjun Song, Jihye Choe, Choong-Heui Chung, Ki-Ha Hong
정지영, 송동준, 최지혜, 정중희, 홍기하
Korean J. Met. Mater. 2019;57(8):535-542.   Published online 2019 Jul 4
DOI: https://doi.org/10.3365/KJMM.2019.57.8.535

Abstract
We investigated the effects of materials and the film thickness of hole transport layers (HTLs) on inverted type perovskite solar cells using optics-charge transport coupled simulations. Power conversion efficiencies (PCEs), and the variations in efficiency induced by the film thickness dispersion, were intensively studied, to compare potential HTLs candidates like..... More

                   Web of Science 3  Crossref 3
Thermal Conductivity of Three-Dimensionally Interconnected Graphene-Networked Cu Composite Fabricated by a Simple Two-Step Process
Xue Li, Terry Arthur Ring, Byung-Sang Choi
Korean J. Met. Mater. 2019;57(8):529-534.   Published online 2019 Jul 11
DOI: https://doi.org/10.3365/KJMM.2019.57.8.529

Abstract
A Cu composite reinforced by a three-dimensionally interconnected graphene network was synthesized in situ by a simple two-step process utilizing compacted Cu powder (99% purity) as a template for the growth of graphene. Cu composites with different graphene contents were obtained by controlling the processing parameters. The composites were approximated..... More

                   Web of Science 6  Crossref 6
Effect of Anodic Oxidation Process Parameters on TiO2 Nanotube Formation in Ti-6Al-4V Alloys
Ti-6Al-4V합금에서 양극산화 공정변수가 TiO2 나노튜브 형성에 미치는 영향
Seung-Yeon Yoo, Hyun Gyoon Park
유승연, 박현균
Korean J. Met. Mater. 2019;57(8):521-528.   Published online 2019 Jul 11
DOI: https://doi.org/10.3365/KJMM.2019.57.8.521

Abstract
To investigate the effect of anodic oxidation process parameters on TiO2 nanotube formation in Ti-6Al-4V alloys, the composition of NH4F and H2O in the anodic oxidation processes were changed under the conditions of constant DC power ranging from 20 V to 60V and current density ranging from 10 mA to..... More

                   Web of Science 4  Crossref 3
Photocatalytic Characterization of TiO2 Nanotubes with Pd Particles Synthesized by Photoreduction Process
광환원반응을 통한 TiO2/Pd 복합광촉매 제조와 광촉매 특성
Jong-Ho Lee, Hong-Joo Ahn, Jeong-Il Youn, Young-Jig Kim, Su-Jeong Suh, Han-Jun Oh
이종호, 안홍주, 윤정일, 김영직, 서수정, 오한준
Korean J. Met. Mater. 2019;57(8):510-520.   Published online 2019 Jul 8
DOI: https://doi.org/10.3365/KJMM.2019.57.8.510

Abstract
To decompose dye in aqueous solution, Pd nanoparticle-decorated TiO2 nanotube photocatalysts were fabricated through electrochemical anodization and photoreduction processes. Morphological and surface characterization of the TiO2/Pd heterojunction photocatalyst, as well as photoelectrochemical behaviors, were investigated by X-ray diffraction, UV/Vis diffuse reflectance and photocurrent response. It was found that the precipitated..... More

                   Web of Science 5  Crossref 3
Separation of Tb(III) and Dy(III) from Chloride Solution by Extraction and Scrubbing with Ionic Liquid Prepared with Cyanex 272 and Aliquat 336
Cyanex 272와 Aliquat 336으로 제조한 이온성액체로 염산용액에서 추출과 세정에 의한 터븀(III) 및 디스프로슘(III)의 분리
Chang Geun Oh, Seong Ho Son, Man Seung Lee
오창근, 손성호, 이만승
Korean J. Met. Mater. 2019;57(8):499-505.   Published online 2019 Jul 8
DOI: https://doi.org/10.3365/KJMM.2019.57.8.499

Abstract
Terbium and dysprosium are rare earth elements which are employed in the manufacture of advanced materials. Separating Tb(III) and Dy(III) is very complicated because their chemical properties are similar. In order to develop a separation process based on solvent extraction, extraction and scrubbing experiments were conducted using weak hydrochloric solutions..... More

                   Web of Science 1  Crossref 1
Effect of Rolling Temperature on the Microstructural Characteristics of High-Speed-Rolled Mg Alloy with Initial Non-Basal Texture
비기저면 집합조직을 가지는 마그네슘 합금의 고속압연 온도 변화에 따른 압연재 미세조직 변화
Su Jin Lee, Ye Jin Kim, Jeong Hun Lee, Sung Hyuk Park
이수진, 김예진, 이정훈, 박성혁
Korean J. Met. Mater. 2019;57(8):482-490.   Published online 2019 Jul 4
DOI: https://doi.org/10.3365/KJMM.2019.57.8.482

Abstract
In this study, the effects of rolling temperature on the microstructural characteristics of a highspeed-rolled Mg alloy with a non-basal texture were investigated. To this end, commercial AZ31 alloy samples in which the basal poles of most grains were tilted at an angle of 45° from the normal direction (ND)..... More

                   Web of Science 2  Crossref 3
Effect of Process Parameters on the Angular Distribution of Sputtered Cu Flux in Long-Throw Sputtering System
Hee-Young Shin, Tae-Ho Kim, Jun-Woo Park, Hyun-Chul Sohn
Korean J. Met. Mater. 2019;57(7):462-467.   Published online 2019 Jun 5
DOI: https://doi.org/10.3365/KJMM.2019.57.7.462

Abstract
In this work, the angular distribution of the sputtered Cu flux in a long throw sputtering (LTS) system is extracted from the comparison of experimentally-measured profiles of deposited films with simulated profiles of films in overhang contact structure. And effects of the sputtering process parameters such as Ar pressure during..... More

                   Web of Science 1  Crossref 1
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